In this work, several dietary supplements extracts were analyzed through HILIC-MS/MS. Via target analyses, legal compounds (sweeteners, methylxanthines) were quantified, while none of the selected illicit substances was detected. Still, a non-target MS study allowed to detect and tentatively identify an analogue of clenbuterol, a prohibited substance.
Target analysis of doping substances and tentative identification of unknowns in dietary supplements through HILIC-MS/MS
Matteo Baglietto;Barbara Benedetti;Marina Di Carro;Emanuele Magi
2023-01-01
Abstract
In this work, several dietary supplements extracts were analyzed through HILIC-MS/MS. Via target analyses, legal compounds (sweeteners, methylxanthines) were quantified, while none of the selected illicit substances was detected. Still, a non-target MS study allowed to detect and tentatively identify an analogue of clenbuterol, a prohibited substance.
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